Response surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS‐SPME-GC-MS

Registro completo de metadados
MetadadosDescriçãoIdioma
Autor(es): dc.creatorZacaroni, Lidiany Mendonça-
Autor(es): dc.creatorSales, Priscila Ferreira de-
Autor(es): dc.creatorCardoso, Maria das Graças-
Autor(es): dc.creatorSantiago, Wilder Douglas-
Autor(es): dc.creatorNelson, David Lee-
Data de aceite: dc.date.accessioned2026-02-09T11:16:38Z-
Data de disponibilização: dc.date.available2026-02-09T11:16:38Z-
Data de envio: dc.date.issued2018-12-28-
Data de envio: dc.date.issued2018-12-28-
Data de envio: dc.date.issued2017-
Fonte completa do material: dc.identifierhttps://repositorio.ufla.br/handle/1/32338-
Fonte completa do material: dc.identifierhttps://onlinelibrary.wiley.com/doi/full/10.1002/jib.410-
Fonte: dc.identifier.urihttp://educapes.capes.gov.br/handle/capes/1137416-
Descrição: dc.descriptionThe extraction of volatile compounds from distilled sugarcane spirits was investigated using central composite design associated with response surface methodology. The parameters evaluated were the extraction temperature, extraction time and desorption time. All of the parameters analysed, as well as their interactions, were significant for the process at a 95% confidence level. Although the extraction time and extraction temperature exhibited positive effects, the desorption time showed a negative effect. The second‐order polynomial model was adjusted appropriately for the response surface analysis. The optimized conditions were extraction temperature equal to 45°C, extraction time of 50 min and the desorption time corresponding to 100 s. Copyright © 2017 The Institute of Brewing & Distilling-
Idioma: dc.languageen-
Publicador: dc.publisherThe Institute of Brewing & Distilling-
Direitos: dc.rightsrestrictAccess-
???dc.source???: dc.sourceJournal of The Institute of Brewing-
Palavras-chave: dc.subjectVolatile compounds-
Palavras-chave: dc.subjectDistilled sugarcane spirits-
Palavras-chave: dc.subjectSolid‐phase microextraction-
Palavras-chave: dc.subjectResponse surface method-
Palavras-chave: dc.subjectCompostos voláteis-
Palavras-chave: dc.subjectAguardente de cana destilada-
Palavras-chave: dc.subjectMicroextração em fase sólida-
Palavras-chave: dc.subjectMétodo de superfície de resposta-
Título: dc.titleResponse surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS‐SPME-GC-MS-
Tipo de arquivo: dc.typeArtigo-
Aparece nas coleções:Repositório Institucional da Universidade Federal de Lavras (RIUFLA)

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