Complete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone.

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MetadadosDescriçãoIdioma
Autor(es): dc.creatorSantos, Marcelo Henrique dos-
Autor(es): dc.creatorNagem, Tanus Jorge-
Autor(es): dc.creatorBraz Filho, Raimundo-
Autor(es): dc.creatorLula, Ivana Silva-
Autor(es): dc.creatorSpeziali, Nivaldo Lucio-
Data de aceite: dc.date.accessioned2025-08-21T15:39:37Z-
Data de disponibilização: dc.date.available2025-08-21T15:39:37Z-
Data de envio: dc.date.issued2017-06-13-
Data de envio: dc.date.issued2017-06-13-
Data de envio: dc.date.issued2001-
Fonte completa do material: dc.identifierhttp://www.repositorio.ufop.br/handle/123456789/7948-
Fonte completa do material: dc.identifierhttp://onlinelibrary.wiley.com/doi/10.1002/mrc.795/full-
Fonte completa do material: dc.identifierhttps://doi.org/10.1002/mrc.795-
Fonte: dc.identifier.urihttp://educapes.capes.gov.br/handle/capes/1020891-
Descrição: dc.descriptionAn NMR study of 15-epiclusianone, 1-benzoyl-6-hydroxy-14,14-dimethyl-3,5,15-tri(3-methyl-2-butenyl)- bicyclo[3.3.1]non-1-ene-4,6-dione (1), a novel tetraisoprenylated benzophenone isolated from pericarp of fruits of Rheedia gardneriana, is described. In addition to conventional 1D NMR techniques, 2D shiftcorrelated NMR experiments [1H 1H-COSY, 1H 13C-HMQC-1J(C,H), 1H 13C-HMBC-nJ(C,H) (n = 2 and 3) and 1H 1H-NOESY] were used for 1H and 13C chemical shift assignments of this natural product. The 1D 13C NMR spectrum of 1 in the solid state was also obtained.-
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Idioma: dc.languageen-
Direitos: dc.rightsrestrito-
Título: dc.titleComplete assignment of the 1H and 13C NMR spectra of the tetraisoprenylated benzophenone 15-epiclusianone.-
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