Structural and vibrational properties of phase - pure monoclinic NdLuO3 interlanthanides synthesized from nanostructured precursors.

Registro completo de metadados
MetadadosDescriçãoIdioma
Autor(es): dc.creatorSoares, Júlia Cristina-
Autor(es): dc.creatorSiqueira, Kisla Prislen Félix-
Autor(es): dc.creatorMoreira, Roberto Luiz-
Autor(es): dc.creatorDias, Anderson-
Data de aceite: dc.date.accessioned2025-08-21T15:10:45Z-
Data de disponibilização: dc.date.available2025-08-21T15:10:45Z-
Data de envio: dc.date.issued2016-07-29-
Data de envio: dc.date.issued2016-07-29-
Data de envio: dc.date.issued2016-
Fonte completa do material: dc.identifierhttp://www.repositorio.ufop.br/handle/123456789/6685-
Fonte completa do material: dc.identifierhttps://doi.org/10.1016/j.jallcom.2016.03.291-
Fonte: dc.identifier.urihttp://educapes.capes.gov.br/handle/capes/1004521-
Descrição: dc.descriptionPhase-pure monoclinic NdLuO3 interlanthanides were successfully synthesized from hydrothermalderived precursors. LuO(OH) and Nd(OH)3 materials were firstly obtained by hydrothermal synthesis at 250 _C, for 24 h. X-ray diffraction, micro-Raman spectroscopy, scanning and transmission electron microscopies were employed to investigate the thermal behavior of these precursors and NdLuO3 interlanthanide up to 1600 _C. It was observed that LuO(OH) and Nd(OH)3 were converted to cubic lanthanide oxides below 1000 _C. Cubic Nd2O3 has changed to the monoclinic structure at 1000 _C, followed by reaction with cubic Lu2O3 at 1400 _C to produce monoclinic NdLuO3. Phase-pure monoclinic (C2/m space group, #12) interlanthanide was then produced at 1600 _C for the first time, as confirmed by all the employed techniques. Phonon modes were additionally determined and assigned for this monoclinic structure.-
Formato: dc.formatapplication/pdf-
Idioma: dc.languageen-
Direitos: dc.rightsaberto-
Direitos: dc.rightsO periódico Journal of Alloys and Compounds concede permissão para depósito deste artigo no Repositório Institucional da UFOP. Número da licença: 3898810936575.-
Palavras-chave: dc.subjectCeramics-
Palavras-chave: dc.subjectElectron microscopy-
Palavras-chave: dc.subjectNanomaterials-
Palavras-chave: dc.subjectRaman spectroscopy-
Palavras-chave: dc.subjectRare earth-
Título: dc.titleStructural and vibrational properties of phase - pure monoclinic NdLuO3 interlanthanides synthesized from nanostructured precursors.-
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