Dereplication of terpenes and phenolic compounds from Inga edulis extracts using HPLC-SPE-TT, RP-HPLC-PDA and NMR spectroscopy

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MetadadosDescriçãoIdioma
Autor(es): dc.contributorUniversidade Estadual Paulista (Unesp)-
Autor(es): dc.contributorScience and Technology of Maranhão-IFMA-
Autor(es): dc.creatorLima, Nerilson M. [UNESP]-
Autor(es): dc.creatorAndrade, Teresinha J. A. S.-
Autor(es): dc.creatorSilva, Dulce Helena S. [UNESP]-
Data de aceite: dc.date.accessioned2022-02-22T00:26:24Z-
Data de disponibilização: dc.date.available2022-02-22T00:26:24Z-
Data de envio: dc.date.issued2020-12-11-
Data de envio: dc.date.issued2020-12-11-
Data de envio: dc.date.issued2019-12-31-
Fonte completa do material: dc.identifierhttp://dx.doi.org/10.1080/14786419.2020.1786824-
Fonte completa do material: dc.identifierhttp://hdl.handle.net/11449/199081-
Fonte: dc.identifier.urihttp://educapes.capes.gov.br/handle/11449/199081-
Descrição: dc.descriptionInga edulis is traditionally used as anti-inflammatory and antidiarrheal and has been investigated as potential sources of biologically active natural products. In this study, dereplication strategy using HPLC-SPE-TT, RP-HPLC-PDA and NMR spectroscopy was employed, and this resulted in the identification of sixteen compounds from the leaves extract of I. edulis, including four triterpenes (lupeol, α-amirin, olean-18-ene acid and frideline), three flavonoids, eight phenolic acids, an anthocyanin derived from delphinidin-3-glycoside and a mixture of five acylated anthocyanins. The chemical identification was performed based on NMR data, chemosystematics aspects, UV spectra and by comparison with the retention time and UV spectra of authentic standards. The metabolic profile of the species indicated the presence of phenolic compounds as major constituents justifying its strong antioxidant potential performed in β-carotene test. The techniques used have shown effective strategies for the early detection of active natural products from plant extracts, as these approaches are still crucially absent. (Figure presented.).-
Descrição: dc.descriptionNucleus of Bioassays Biosynthesis and Ecophysiology of Natural Products (NuBBE) Institute of Chemistry São Paulo State University (UNESP)-
Descrição: dc.descriptionNucleus of Applied Research to Sciences-NIAC Federal Institute of Education Science and Technology of Maranhão-IFMA-
Descrição: dc.descriptionNucleus of Bioassays Biosynthesis and Ecophysiology of Natural Products (NuBBE) Institute of Chemistry São Paulo State University (UNESP)-
Idioma: dc.languageen-
Relação: dc.relationNatural Product Research-
???dc.source???: dc.sourceScopus-
Palavras-chave: dc.subjectdereplication-
Palavras-chave: dc.subjectHPLC-SPE-TT-
Palavras-chave: dc.subjectInga edulis-
Palavras-chave: dc.subjectMedicinal plants-
Palavras-chave: dc.subjectNMR-
Palavras-chave: dc.subjectRP-HPLC-PDA-
Título: dc.titleDereplication of terpenes and phenolic compounds from Inga edulis extracts using HPLC-SPE-TT, RP-HPLC-PDA and NMR spectroscopy-
Tipo de arquivo: dc.typelivro digital-
Aparece nas coleções:Repositório Institucional - Unesp

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